Pope Scientific has released a case study of its collaboration with AB Specialty Silicones to optimize process and product quality.
AB Specialty Silicones is a U.S. manufacturer and worldwide distributor of specialty silicone chemicals.
AB’s core brand, Andisil, encompasses a broad product catalog serving many industries including personal care, dental & medical, specialty chemical manufacturing, electronic encapsulation, adhesives & sealants, coatings, mold making, gypsum, mineral & fiber treatment, pulp manufacturing, roof coatings and others.
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One of several factors in common with the highest quality polymers, including silicones, is having a very low amount of residual volatiles.
In the early stages of product development, AB Specialty Silicones reached out to Pope Scientific to explore the best methods for producing low volatile silicone pre-polymers and polymers.
Specifically, AB needed to respond to the demand for volatile-free silicone polymers for encapsulation in the LED industry. This particular application brought unique challenges.
Silicones can be heat sensitive, leading to degradation including color change, (prohibited for LED applications). Typical batch mode boiling vessel methods for removal of cyclics and monomers were causing such degradation due to the long residence heating time of many hours.
After Pope spent some time learning about the specifics of the application and its challenges, they collaborated with AB to develop the best method with strategies for optimizing the end product through lab trials and pilot plant process development.
By utilizing short-path molecular distillation with Pope’s wiped-film still technology, the potential for final product degradation and discoloration is greatly reduced or eliminated through efficient equipment and design process, high vacuum and decreasing the heat exposure time to a matter of seconds.
Once the processing techniques were finalized, Pope began production toll processing campaigns of the material in their Saukville, WI, facility.
Bill Marman, Pope’s tolling supervisor, was essential in aiding AB with process development and support throughout this initial project, as well as with future projects.
“The original tolling run produced around 40 drums of the specialty low volatile silicone polymers,” said Mac Penman, AB Specialty Silicones’ general manager.
In 2009, Pope built AB, a 9” wiped-film distillation system to run in-house at their Waukegan, IL facility.
Pope helped AB commission the system and was there throughout the installation, performing final equipment testing, process startup and training. They were able to duplicate the processing in-house that they previously had to contract out.
“There has always been an open dialogue with Pope. From pricing, to engineering and sales, we’ve gotten great support. We have a great relationship,” says Penman.
The new equipment provided AB the ability to increase production of specialty chemicals, often times with complex distillation requirements, for their customers.